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<div id="vuors3fz7odt" class="appContent"> <div id="vuors3fz7odt" class="datum_info"> <h1 class="title">如何用藥水來辨彆西安大口徑不鏽鋼管材料的真?zhèn)?/h1> <div id="vuors3fz7odt" class="bgcolor_01"> <div id="vuors3fz7odt" class="bgcolor_sum"> <div id="vuors3fz7odt" class="left">日期：2025-04-21 10:18</div> <div id="vuors3fz7odt" class="right">瀏覽次數(shù)：866</div> </div> <div id="vuors3fz7odt" class="bgcolor_sum01"> 摘要： </div> </div> <div id="vuors3fz7odt" class="content"> <div>如何用藥水來辨彆<a href="http://m.txcc.com.cn/timemodel/firstctg/2013-09-30/3140739/1.html ">西安大口徑不鏽鋼管</a>材料的真?zhèn)?/div><div>一、測試方法簡介</div><div>1、大口徑不鏽鋼管中含鐵是用千分之為單位，鎳量是用百分之為單位這是測出來的可以用光譜分析來測。大口徑不鏽鋼管中鎳含量的測定除了分光光度法，EDTA滴定法和丁二酮肟重量法了解丁二酮肟鎳重量法測定鎳的原理和方法，掌握用玻璃坩堝過濾等重量分析法基本操作。</div><div>丁二酮肟是二元弱酸（以H2D表示），其分子式為C4H8O2N2，摩爾質(zhì)量為1162g??mol-1。研究表明，隻有HD-狀態(tài)才能在氨性溶液中與Ni2+發(fā)生沉澱反應(yīng)：經(jīng)過濾，洗滌，在120℃下烘乾至恒重，稱得丁二酮肟鎳沉澱的質(zhì)量mNi(HD)2,以下式計算Ni的質(zhì)量分?jǐn)?shù)：ωNi=本法沉澱介質(zhì)的酸度為pH=8～9的氨性溶液。酸度大，生成H2D，使沉澱溶解度增大，酸度小，由於生成D2-，同樣將增加沉澱的溶解度。氨濃度太高，會生成Ni2+的氨絡(luò)合物。</div><div>丁二酮肟是一種高選擇性的有機(jī)沉澱劑，它隻與Ni2+，Pd2+，F(xiàn)e2+生成沉澱。Co2+，Cu2+與其生成水溶性絡(luò)合物，不僅會消耗H2D，且會引起共沉澱現(xiàn)象。當(dāng)Co2+，Cu2+含量高時，*好進(jìn)行二次沉澱或預(yù)先分離。</div><div>由於Fe3+，Al3+，Cr3+，Ti4+等離子在氨性溶液中生成氫氧化物沉澱，乾擾測定，故在溶液加氨水前，需加入檸檬酸或酒石酸絡(luò)合劑，使其生成水溶性的絡(luò)合物。<br> <br>主要試劑和儀器 <br>1. 混合酸HCl+HNO3+H2O （3+1+2） <br>2. 酒石酸或檸檬酸溶液(500g??L-1) <br>3. 丁二酮肟(10g??L-1)乙醇溶液 <br>4. 氨水（1+1） <br>5. HCl（1+1） <br>6. HNO3(2mol??L-1) <br>7. AgNO3(0.1mol??L-1) <br>8. 氨-氯化銨洗滌液：每100mL水中加入1mL氨水和1g NH4Cl。 <br>9. G4號微孔玻璃坩堝 <br>10. 鋼鐵試樣</div><div><span style="color: #993300">公司至成立以來，以“誠信、合作、雙贏、發(fā)展”為經(jīng)營宗旨，堅持“價格*優(yōu)、用戶、信譽(yù)”的營銷理念，在市場上獲得了良好的口碑。 029—88633755<br></span>詳情參考：<a href="http://m.txcc.com.cn/">http://m.txcc.com.cn</a></div><div> </div> </div> <div id="vuors3fz7odt" class="datumrelate"> <span>下一篇：</span> <a href="/zh-tw/timemodel/news/2014-03-22/951339.html" title="西安不鏽鋼管的切削特點(diǎn)">西安不鏽鋼管的切削特點(diǎn)</a> <br> <span>上一篇：</span> <a href="/zh-tw/timemodel/news/2014-03-23/951690.html" title="西安不鏽鋼管的壁厚精度要求 ">西安不鏽鋼管的壁厚精度要求 </a> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> </div> <div class="vuors3fz7odt" id="layout_04001205_style" class="hide"> </div> </div> </div> </div> <footer id="footer" class="footer" data-appid="layout"> <div class="vuors3fz7odt" id="footerWrapper" class="footerWrapper" data-appid="wrapper"> <div class="vuors3fz7odt" id="footerContainer" class="footerContainer" data-appid="container"> <div 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